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SS2100 - CO2 Bulk Gas in N2/H2/Ar/He/CO2

Measure Carbon Dioxide in Bulk Gases using Tunable Diode Laser technology, a maintenance-free alternative to traditional moisture monitors.
Product Code: 65303
 
 
 
 
 

Application Note

Bulk Compressed Gases
Carbon Dioxide is one of the most important impurities in high purity gases such as Nitrogen, Helium, Hydrogen and Argon.

Critical Control of Carbon Dioxide
Some of these bulk gases are manufactured by cryogenic processes. Others are cleaned of CO2 using fixed bed molecular sieves or acid gas absorbents as part of the process. In any case, the CO2 content of the gas must be measured to ensure purity of the final product.

Traditional Measurement Solutions
Trace gas analyzers based on chromatographic separations and helium ionization type detectors have been used, but the detectors required are notoriously sensitive to ambient air leaks in permeation in the columns and fittings, so that maintenance is often a problem. Methanation and measurement by Flame Ionization detectors is one approach, but the high cost of consumables, such as columns, valves, carrier and detector gases makes the cost of these analyzer prohibitive, and GC measurements are inherently slow. Non-dispersive IR methods can be used, but long, folded-path cells to achieve the sensitivity required are expensive and the measurement is prone to interferences.

SpectraSensors’ Solution
SpectraSensors SS2100 is the ideal solution for bulk gas applications. Tunable Diode Laser technology means measurement interferences from other infrared absorbing compounds are avoided. There are no wet-up or dry-down delays, resulting in fast updates even when the concentration changes dramatically. The calibration is stable over the life of the analyzer. There are no consumable parts or supplies. The analyzer is virtually maintenance free and has a low cost of ownership.

Validation
The CO2 measurements can be validated using a certified standard of CO2 in a balance of Nitrogen.
 
Typical Stream Composition

Component

Unit

Typical Concentration

Min. for Application

Max. for Application

Carbon Dioxide (CO2)

ppmv

100

4

1000

H2O

Mole%

<0.01

0

0.5

Nitrogen (N2)

Mole%

99.99+

98.0

100

Helium (He)

Mole%

99.99+

98.0

100

Hydrogen (H2)

Mole%

99.99+

98.0

100

Argon (Ar)

Mole%

99.99+

98.0

100

Total

Mole%

100

 

 

 

The background stream composition must be specified for proper calibration and measurement performance. If other than a high purity gas, please specify the normal composition, along with the minimum and maximum expected values for each component, especially CO2, the measured component. Other stream compositions may be allowable with approval from SpectraSensors. 


 

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Data Sheet


Performance

Target Components

CO2 in Compressed Gases (N2/H3/H2/Air)
Specify Background Gas

Typical Measurement Ranges

≥0 – 200 ppm*
(specify range)

Typical Precision

 ±2% of Full Scale

Measurement Response Time

1 to ~60 sec*

Principle of Measurement

Tunable Diode Laser Absorption Spectroscopy
Non-differential

Environmental Temperature Range

-20º to 50ºC (-4º to 122ºF)
-10º to 60ºC (14º to 140ºF) optional

Sample Inlet Pressure

70 kPag (10 psig) typical

210 kPag (30 psig) maximum


Cell Temperature

Maintain at 50ºC +/- 0.2ºC

Maximum Cell Pressure

70 kPag (10 PSIg)

Sample Flow Rate
 
3 - 4 L/min (6.4 to 8.5 scfh)*
Validation
Certified blend of CO2 in Nitrogen balance
 

Electrical

Power

100-240 VAC, 50-60 Hz standard

Max Current

Controller: 1 A @ 120 VAC

Controller to Cell Cable Length

1m standard (3m, 5m & 10m available optionally)

Communication

Current Loop Output 4-20 mA Isolated, 1200 ohms @ 24 VDC max load
Serial: ASCII Text RS232C standard
Modbus RS232C
Digital Outputs
4 ea. 12 VDC for valve operations
Scrubber (if required), Process/Val, Val 1, Val 2
5 SPDT (Form C) Dry Contact Alarms
Common Fault, Val 1 Active, Val 2 Active, Val Fail,
one user-assignable to any alarm 
LCD Display
Concentration, Cell Pressure and Temperature, Diagnostic Data
 

Physical

Controller Enclosure

NEMA 4X - 304 Stainless Steel standard

Controller Dimensions

343mm H x 305mm W x 165mm H
(13.5" H x 12" W x 6-7/16" D)*

Weight Approximately

13.1 Kg (28.6 lbs)*

Sample Cell Dimensions

8m Herriot Cell
559 mm H × 127 mm W
(22” H × 5” W)

Sample Cell Construction

316L Series Polished Stainless Steel standard
Number of Sample Cells
1 (single channel SS2100) or
2 (dual channel SS2100)
Area Classification
CSA Certified for Class I, Division 2,
Groups ABCD Temp Code T3C
 ll 2G Ex d llB+H2 T5; Tamb : -20 ÷ +60 °C
Dimensions with Sample System 1678 mm H x 613 mm W x 427 mm D
(66” H x 24-1/8” W x 16-13/16” D)
Weight with Sample System (approx.) 68 kg (150 lbs.)

* Application specific; consult factory

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Drawings


Typical Accessories


SS2100 ARM9 Electronics
 

80000-02199

Temperature Control Board

23000-00030

4-20 mA Current Loop Board
 

80000-02203

Power Supply Assembly, 120/240 VAC 50/60 Hz
 

80000-02300

Power Supply Assembly, 24 VDC
 

01902-17106 External Serial Output Cable

01902-30011 Keypad Assembly

24601-00002
Display Assembly
 
02203-13100
Daughter Board
 
45000-02002
Relay, DC12V SPDT 3 A/120 VAC
 

Herriott Cell (8m & 28m)
02101-17102
Pressure Transducer Assembly
 
02101-17103
Thermistor Assembly
 
02199-00006
Spares Kit (o-rings, fuses), AC, Viton
 
02199-00007
Cleaning Kit (domestic only)
 
 
 

Photos

 
 

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